Abstract
The crystalline trichloro
compound obtained from sclareol (I), manool (VI), and the manoyl oxides (IX, X)
by addition of hydrogen chloride has the 8R,13,16-trichlorolabdane structure
(XII). The compound is a 1 : 1 mixture of C13 epimers which are inseparable by
normal means. However, addition of the trichloride to an equal amount of the
antipodal mixture obtained from the enantiomeric manoyl oxide [(-)X] readily
gave two separable racemates.
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