Direct Introduction of Steel Samples into a Capacitively Coupled Microwave Plasma for Atomic Emission Spectrometry

Author:

Masamba Wellington R. L.1,Smith Benjamin W.1,Winefordner James D.1

Affiliation:

1. Department of Chemistry, University of Florida, Gainesville, Florida 32611

Abstract

The feasibility of analyzing steel samples by direct introduction into a helium/hydrogen mixed-gas capacitively coupled microwave plasma was assessed with steel standard reference materials (NIST 442-450). Linear calibration curves were obtained for various concentration ranges. Limits of detection for Sn and Pb were 5 μg/g and 0.08 μg/g, respectively.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

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