Crystal structure, microstructure, and magnetic properties of the Fe2CrSi nanostructured Heusler alloy elaborated by the mechanical alloying method

Author:

Djaidi Fatiha1,Mechri Hanane2,Azzaz Mohammed2

Affiliation:

1. USTHB BP 32 EL ALIA Bab Ezzouar, Algiers , Algeria

2. Laboratory of Materials Science and Engineering, University of Science and Technology Houari Boumediene (USTHB), Algiers , Algeria

Abstract

Abstract The Fe2CrSi nanostructured Heusler alloy was prepared by mechanical alloying followed by heat treatment. The structure, microstructure, and magnetic properties of the samples were studied by the following analysis methods: X-ray diffraction, scanning electron microscopy with energy dispersive X-ray spectrometry, transmission electron microscopy, and a vibrating sample magnetometer. The a-Fe (Si, Cr) solid solution with a disordered body centered cubic (bcc) crystal structure was obtained after 24 h of milling. An example of the sample milled for 32 h with a disordered crystal structure a-Fe(Si, Cr) was chosen to investigate the transformation with temperature using differential scanning calorimetry. The effect of annealing temperatures on the structural, microstructural, and magnetic properties of the ordered Fe2CrSi Heusler phase for the sample milled for 32 h was investigated.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,Metals and Alloys,Physical and Theoretical Chemistry,Condensed Matter Physics

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