Step-flow growth of Al droplet free AlN epilayers grown by plasma assisted molecular beam epitaxy

Author:

Shao Pengfei,Li Siqi,Li Zhenhua,Zhou Hui,Zhang Dongqi,Tao Tao,Yan Yu,Xie Zili,Wang KeORCID,Chen DunjunORCID,Liu BinORCID,Zheng Youdou,Zhang Rong,Lin Tsungtse,Wang Li,Hirayama Hideki

Abstract

Abstract We have investigated an Al modulation epitaxy (AME) method to obtain step-flow growth of Al droplet free AlN layers by plasma assisted molecular beam epitaxy (MBE). At the usual growth temperature of (Al)GaN/AlN heterostructures, Al atom migration and desorption rate are very low and consequently it is very difficult to avoid the formation of Al droplets on AlN growth front by conventional MBE growth method. By adopting the AME growth method, such a difficulty has been effectively overcome and step flow growth mode of AlN has been clearly observed. By optimizing the AME growth time sequence, namely, AlN growth time and N radical beam treatment time, Al droplet free AlN layers with step flow growth characteristics have been obtained, with atomic flat surfaces and an average atomic step width of ∼118 nm at 970 °C–1000 °C, which is still suitable to grow (Al)GaN/AlN heterostructures by MBE.

Funder

National Key R&D Program of China

National Nature Science Foundation of China

Jiangsu Special Professorship

Collaborative Innovation Center of Solid State Lighting and Energy-saving Electronics

Key R&D Program of Jiangsu province

Fundamental Research Funds for the Central Universities

Publisher

IOP Publishing

Subject

Surfaces, Coatings and Films,Acoustics and Ultrasonics,Condensed Matter Physics,Electronic, Optical and Magnetic Materials

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