Quantitative analysis by Raman spectroscopy using potassium hexacyanoferrate (III) as an internal standard-Reference-Cited by-同舟云学术

Quantitative analysis by Raman spectroscopy using potassium hexacyanoferrate (III) as an internal standard

Published:2020-03-07 Issue:1 Volume: Page:13-16
ISSN:2686-701X
Container-title:Agrarian science
language:
Short-container-title:Agrarnaâ nauka

Author:

Khrushchev A. Y.¹,Akmaev E. R.¹,Bondarenko V. O.¹,Metlin A. E.¹

Affiliation:

1. The Russian State Center for Animal Feed and Drug Standardization and Quality

Abstract

In this article we proposed a method for quantitative determination of active substance in pharmaceuticals via Raman scattering using potassium ferricyanide as internal standard. We approved this method in ketoprophenum quantitative determination in drug for veterinary use “Ketojekt”. The calculation of metrological requirements of procedures are established proposed method of calibration. Either we demonstrated the focalisation factor of laser beam affects on the method reproducibility. The method provides a precise, rapid, convenient to quantitative analysis that is more effective than the standard HPLC assay.

Publisher

Agrarian Science

Reference16 articles.

1. M. R. Witkowski, American pharmaceutical review, Volume 8, Issue 1, 56-62 (2005).

2. M. Otsuka, Y. Fukui, K. Otsuka, et al., J.Near Infrared Spectroscopy, 14(1), 9-16 (2006).

3. O. Kolomiets, U. Hoffmann, P. Geladi, et al., Applied spectroscopy, 62 (11), 1200-1208 (2008).

4. D.A. Burns and E.W. Ciurczak (Eds.), Handbook of NearInfrared analysis, Second edition, Marcel Dekker Inc, New York Basel, (2001), pp. 53-70.

5. E.W. Ciurczak and B. Igne (Eds.), Pharmaceutical and Medical Applications of Near-Infrared Spectroscopy, Second edition, CRC, Boca Raton, (2014), pp. 73-96