Redetermination of the crystal structure of (2E,4Z,13E,15Z)-3,5,14,16-tetramethyl-2,6,13,17-tetraazatricyclo[16.4.0.07,12]docosa-1(22),2,4,7,9,11,13,15,18,20-decaene, C22H24N4-Reference-Cited by-同舟云学术

Redetermination of the crystal structure of (2E,4Z,13E,15Z)-3,5,14,16-tetramethyl-2,6,13,17-tetraazatricyclo[16.4.0.07,12]docosa-1(22),2,4,7,9,11,13,15,18,20-decaene, C22H24N4

Published:2021-07-21 Issue:5 Volume:236 Page:1121-1124
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Dey Lucky¹,Rabi Saswata¹²,Begum Zinnat A.³⁴^ORCID,Takase Tsugiko⁵,Rahman Ismail M. M.³^ORCID,Tiekink Edward R. T.⁶^ORCID,Roy Tapashi Ghosh¹

Affiliation:

1. Department of Chemistry , Faculty of Science, University of Chittagong , Chattogram 4331 , Bangladesh

2. Department of Chemistry , Faculty of Engineering & Technology, Chittagong University of Engineering & Technology , Chattogram 4349 , Bangladesh

3. Institute of Environmental Radioactivity, Fukushima University , 1 Kanayagawa, Fukushima City , Fukushima 960-1296 , Japan

4. Department of Civil Engineering , Southern University Bangladesh , Arefin Nagar, Bayezid Bostami , Chattogram 4210 , Bangladesh

5. Department of Natural Sciences and Informatics , Fukushima University , 1 Kanayagawa , Fukushima 960-1296 , Japan

6. Research Centre for Crystalline Materials, School of Science and Technology, Sunway University , 47500 Bandar Sunway , Selangor Darul Ehsan , Malaysia

Abstract

Abstract C22H24N4, triclinic, P 1 ‾

$P‾{1}$

(no. 2), a = 9.217(4) Å, b = 9.774(4) Å, c = 10.843(4) Å, α = 96.770(2)°, β = 101.791(5)°, γ = 105.873(3)°, V = 903.9(6) Å3, Z = 2, R gt (F) = 0.0391, wR ref (F 2) = 0.1069, T = 93(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2021-0244/pdf

Reference23 articles.

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4. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

5. Farrugia, L. J. WinGX and ORTEP for Windows: an update. J. Appl. Crystallogr. 2012, 45, 849–854; https://doi.org/10.1107/s0021889812029111.

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