Crystal structure of (5R,6S,E)-5-acetoxy-2-methyl-6-((2aR,3R,5aS,5bS,11aR,12aS)-2a,5a,8,8-tetramethyl-9-oxotetradecahydro-1H,12H-cyclopenta[a]cyclopropa[e]phenanthren-3-yl)hept-2-enoic acid, C32H48O5

Author:

Li Ting-Kai1,Xiao Li1,Wei Peng1ORCID,Ye Jiang-Hai1,Zhao Chen-Liang1,He Kang1,Zou Juan1

Affiliation:

1. Guizhou University of Traditional Chinese Medicine , Guiyang 550025 , P.R. China

Abstract

Abstract C32H48O5, orthorhombic, P212121 (no. 19), a = 7.1564(10) Å, b = 17.542(3) Å, c = 23.134(4) Å, V = 2904.2(8) Å3, Z = 4, Rgt (F) = 0.0555, wRref (F 2) = 0.1343, T = 273(2) K.

Funder

National Natural Science Foundation of China

Natural-Scientific Research Program of Department of Education of Guizhou Province, Qianjiaoji

Publisher

Walter de Gruyter GmbH

Reference12 articles.

1. Dolomanov, O. V.; Bourhis, L. J.; Gildea, R. J.; Howard, J. A. K.; Puschmann, H. OLEX2: A Complete Structure Solution, Refinement and Analysis Program. J. Appl. Crystallogr. 2009, 42, 339–341.

2. Bruker. APEX2, SAINT and SADABS; Bruker AXS Inc.: Madison, Wisconsin, USA, 2012.

3. Sheldrick, G. M. Crystal Structure Refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Pan, L. T. Medicinal Fern Plants in Guizhou; Guizhou Science and Technology Publishing House: Guiyang, China, 2012.

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