Crystal structure of [(μ2-succinato κ3 O,O′:O′′)-bis-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)]dinickel(II)] diperchlorate, dihydrate C36H82Cl2N8Ni2O15-Reference-Cited by-同舟云学术

Crystal structure of [(μ2-succinato κ3 O,O′:O′′)-bis-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)]dinickel(II)] diperchlorate, dihydrate C36H82Cl2N8Ni2O15

Published:2021-01-22 Issue:3 Volume:236 Page:491-493
ISSN:2197-4578
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Li Wen-Yi¹,Ou Guang-Chuan²^ORCID

Affiliation:

1. Key Laboratory of Functional Metal-Organic Compounds of Hunan Province, College of Chemistry and Materials Science, Hengyang Normal University , HengYang , Hunan 421008 , P. R. China

2. Department of Biology and Chemistry , Hunan University of Science and Engineering , Yongzhou , Hunan 425199 , P. R. China

Abstract

Abstract C36H82Cl2N8Ni2O15, monoclinic, P21/n (no. 14), a = 17.657(3) Å, b = 16.047(3) Å, c = 18.346(3) Å, β = 109.062(4)°, V = 4913.2(16) Å3, Z = 4, R gt (F) = 0.0561, wR ref (F 2) = 0.1664, T = 173(2) K.

Funder

NSFC

Scientific Research Hunan Provincial Education Department

Foundation of Key Laboratory of Functional Metal-Organic Compounds of Hunan Province

Foundation of Hengyang Normal University

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2020-0616/pdf

Reference6 articles.

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System (ver. 4.0); Crystal Impact: Bonn, Germany, 2015.

5. Jiang, L., Feng, X. L., Lu, T. B. Supramolecular architectures of macrocyclic nickel(II) complexes with defined structures of cis and trans configurations. Cryst. Growth Des. 2005, 5, 1469–1475; https://doi.org/10.1021/cg049559r.