The crystal structure of ethyl 2,3,5-trifluoro-4-(4-oxo-3,4-dihydropyridin-1(2H)-yl)benzoate, C14H12F3NO3-Reference-Cited by-同舟云学术

The crystal structure of ethyl 2,3,5-trifluoro-4-(4-oxo-3,4-dihydropyridin-1(2H)-yl)benzoate, C₁₄H₁₂F₃NO₃

Published:2022-09-09 Issue:6 Volume:237 Page:1087-1089
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Wang Jingjing¹,Wu Yundeng²^ORCID,Li Yong³

Affiliation:

1. Department of Student Affairs , Ningbo Polytechnic , No. 388, Lushan East Road, Ningbo Economic and Technological Development Zone, Beilun District , Ningbo City 315806 , Zhejiang Province , P. R. China

2. Technique Center , Jinling Pharmaceutical Company Limited , Nanjing 210046 , Jiangsu Province , P. R. China

3. School of Chemical Engineering , Ningbo Polytechnic , No. 388, Lushan East Road, Ningbo Economic and Technological Development Zone, Beilun District , Ningbo City 315806 , Zhejiang Province , P. R. China

Abstract

Abstract C14H12F3NO3, monoclinic, P21/n (no. 14), a = 14.4583(12) Å, b = 6.6553(5) Å, c = 14.8395(11) Å, β = 113.733(3)°, V = 1307.16(18) Å3, Z = 4, Rgt (F) = 0.0479, wRref (F 2) = 0.1235, T = 170 K.

Funder

School of Chemical Engineering, Ningbo Polytechnic

Ningbo Polytechnic Zhejiang Collaborative Innovation Center

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0412/pdf

Reference20 articles.

1. Bruker. SMART and SAINT; Bruker AXS Inc.: Madison, WI, USA, 2014.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. Morgan, M. M., Marwitz, A. J. V., Piers, W. E., Parvez, M. Comparative lewis acidity in fluoroarylboranes: B(o–HC6F4)3, B(p–HC6F4)3, and B(C6F5)3. Organometallics 2013, 32, 317–322; https://doi.org/10.1021/om3011195.