Crystal structure of hexakis(μ2-azido-κ2N:N)-diazido-κ1N-tetrakis(phenanthroline-κ2N,N′)tetrazinc(II), C48H32N32Zn4

Author:

Feng Yu-Quan1,Zhong Zhi-Guo1,Yue Zi-Long1

Affiliation:

1. College of Chemistry and Pharmacy Engineering, Nanyang Normal University, Nanyang 473061, China

Abstract

AbstractC48H32N32Zn4, triclinic, P1̄ (no. 2), a = 9.9928(14) Å, b = 10.1374(14) Å, c = 14.2362(19) Å, α = 71.710(2)°, β = 76.166(2)°, γ = 71.086(2)°, V = 1280.1(3) Å3, Z = 1, Rgt(F) = 0.0314, wRref(F2) = 0.0795, T = 296(2) K.

Funder

National Natural Science Foundation of China

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference14 articles.

1. A novel dinuclear bismuth(III) coordination compound: bis(μ-pyridine-2,6-dicarboxylato)-κ4O2,N, O6:O6′;κ4O2:O2′,N,O6-bis[(azido-κN)(1,10-phenanthroline-κ2N,N′)bismuth(III)]tetrahydrate;Acta Crystallogr,2014

2. Crystal structure refinement with SHELXL;Acta Crystallogr,2015

3. Structural and magnetic properties of three one-dimensional azido-bridged copper(II) and manganese(II) coordination polymers;Inorg. Chem,2003

4. Di-μ-1,1-azido-bis[azido(5,5′-dimethyl-2,2′-bipyridine-κ2N,N′)zinc(II)];Acta Crystallogr,2007

5. OLEX2: a complete structure solution, refinement and analysis program;J. Appl. Crystallogr,2009

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