Synthesis and structure refinement of the zinc hydroxide boracite: Zn3B7O13(OH)-Reference-Cited by-同舟云学术

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Synthesis and structure refinement of the zinc hydroxide boracite: Zn₃B₇O₁₃(OH)

Published:2024-01-01 Issue:1 Volume:79 Page:51-55
ISSN:0932-0776
Container-title:Zeitschrift für Naturforschung B
language:en
Short-container-title:

Author:

Ziegler Raimund¹,Jungmann Sabrina¹,Huppertz Hubert¹

Affiliation:

1. Department of General, Inorganic, and Theoretical Chemistry , University of Innsbruck , Innrain 80–82, A-6020 Innsbruck , Austria

Abstract

Abstract The new zinc borate Zn3B7O13(OH) crystallizes trigonally in the space group R3c (no. 161) with the lattice parameters a = 849.76(3), c = 2099.8(2) pm, V = 1.3131(2) nm3, and six formula units per unit cell (Z = 6). It was synthesized at high-pressure/high-temperature conditions in a multianvil device. Single-crystal and powder X-ray diffraction experiments were conducted.

Publisher

Walter de Gruyter GmbH

Link

https://www.degruyter.com/document/doi/10.1515/znb-2023-0096/pdf

Reference35 articles.

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2. Schnelle, W., Schmid, H. Phys. Rev. B 2015, 91, 184411.

3. Fouassier, C., Levasseur, A., Joubert, J. C., Muller, J., Hagenmuller, P. Z. Anorg. Allg. Chem. 1970, 375, 202–208; https://doi.org/10.1002/zaac.19703750210.

4. Jeitschko, W., Bither, T. A. Z. Naturforsch. 1972, 27b, 1423.

5. Jeitschko, W., Bither, T. A., Bierstedt, P. E. Acta Crystallogr. 1977, B33, 2767–2775.

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