Affiliation:
1. Institut für Anorganische und Analytische Chemie der Technischen Universität Braunschweig, Pockelsstraße 4, D-3300 Braunschweig
2. Gesellschaft für Biotechnologische Forschung mbH, Mascher oder Weg 1, D-3300 Braunschweig-Stöckheim
Abstract
Abstract
The 2,2,5,5-tetraorganyl-1,4-dioxa-2,5-disilacyclohexanes 2a-2c were prepared by condensation of the corresponding (hydroxymethyl)diorganylsilanes 1 a-1 c. The constitution of the heterocycles was confirmed by elemental analyses, cryoscopic measurements, mass spectrometry, and NMR-spectroscopic (1H, 13C) investigations. The molecular structure of 2 b was determined by X-ray diffraction analysis.
Cited by
9 articles.
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1. Polysilanes, Polycarbosilanes, Dioxadisilacyclohexane, and Polysiloxanes;Efficient Methods for Preparing Silicon Compounds;2016
2. CHR-Insertion (RH, CH3) into Cyclohexyl-Substituted Silsesquioxanes: Reactivity and Decomposition Studies;Chemistry - A European Journal;2014-09-01
3. Synthesis of 2,2,5,5-Tetrasubstituted 1,4-Dioxa-2,5-disilacyclohexanes via Organotin(IV)-Catalyzed Transesterification of (Acetoxymethyl)alkoxysilanes;Chemistry - A European Journal;2013-02-18
4. Baseinduzierte 1,3-Si, O-Trimethylsilylwanderung in α-Hydroxyalkylpolysilanen;Zeitschrift für Chemie;2010-08-31
5. Metabolites of Hexamethyldisiloxane and Decamethylcyclopentasiloxane in Fischer 344 Rat Urine—A Comparison of a Linear and a Cyclic Siloxane;Drug Metabolism and Disposition;2003-02-01